Analysis of polychlorinated biphenyls in cream and ice cream using modified QuEChERS extraction and GC?QqQ?MS/MS method: A risk assessment study

نویسندگان

چکیده

The concentrations of six non–dioxin-like polychlorinated biphenyls (NDL-PCBs) were measured using the quick, easy, cheap, effective, rugged, and safe (QuEChERS) by gas chromatography (GC) coupled with triple-quadrupole (QqQ) tandem mass spectrometry (MS/MS) method in cream ice offered Tehran (Iran). results showed limits detection, limit quantification recovery for PCB analytes ranges 0.04–0.16, 0.132–0.482 ng/g fat, 5.2–9.2 95.5–107.2%, respectively. mean concentration total 6NDL-PCBs (21.634 ± 2.18 fat) was higher than that (12.317 1.524 samples. estimated daily intake (EDI) lower tolerable (TDI < 10 ng/kg BW/day). Ultimately, probabilistic model Monte Carlo simulation (MCS) revealed incremental lifetime cancer risk levels (95th) compounds (adults = 1.62E?6 children 4.37E?6) 9.65E?7 7.57E?6) level acceptable (10?4).

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ژورنال

عنوان ژورنال: International Journal of Dairy Technology

سال: 2022

ISSN: ['1471-0307', '1364-727X']

DOI: https://doi.org/10.1111/1471-0307.12849