Crambin - record in crystallographic resolution for a biological macromolecule

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On the direct determination of three-dimensional crystallographic phases at low resolution: crambin at 6 A.

Using a pseudo-atom approach, the three-dimensional crystallographic phases for the protein crambin (a = 40.76, b = 18.49, c = 22.33 A, beta = 90.61 degrees, space group P2(1)) were determined to 6 A by direct methods. First, the centrosymmetric h0l set was assigned phases by symbolic addition, and the initial solution was then refined by Fourier methods. Phase values of strong reflections were...

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ژورنال

عنوان ژورنال: Acta Crystallographica Section A Foundations and Advances

سال: 2014

ISSN: 2053-2733

DOI: 10.1107/s205327331408797x