Observation of Diffusive Flows during Liquid Phase Microwave Sintering

Solid Solution Formation during Liquid Phase Sintering

Evaluation of Heterogeneous Densification, Anisotropic Shrinkage and Rheological Behavior of Ceramic Materials during Liquid Phase Sintering by Numerical-Experimental Procedure

The effective shear and bulk viscosity, as well as dynamic viscosity, describe the rheological properties of the ceramic body during the liquid phase sintering process. The rheological parameters depend on the physical and thermo-mechanical characteristics of the material such as relative density, temperature, grain size, diffusion coefficient, and activation energy. Thermal behavior of the cer...

Discussion on Microwave-Matter Interaction Mechanisms by In Situ Observation of “Core-Shell” Microstructure during Microwave Sintering

This research aims to deepen the understanding of the interaction mechanisms between microwave and matter in a metal-ceramic system based on in situ synchrotron radiation computed tomography. A special internal "core-shell" microstructure was discovered for the first time and used as an indicator for the interaction mechanisms between microwave and matter. Firstly, it was proved that the microw...

Finite element simulation of pyroplastic deformation, anisotropic shrinkage and heterogeneous densification for ceramic materials during liquid phase sintering process

Pyroplastic deformation is a distortion of the ceramic shape during the sintering process. It occurs because the flow of the vitreous phase at high temperature and the applied stress due to the weight of the product during sintering process. The aim of this paper deals with describing a numerical-experimental method to evaluate the pyroplastic deformation, to predict the anisotropic shrinkage a...

Microwave Sintering of Mullite

Microwave sintering possesses unique attributes and has the potential to be development as a new technique for controlling microstructure and to improve the properties of advanced ceramics. Because microwave radiation penetrates most ceramics, uniform volumetric heating is possible. Thermal gradients, which are produced during conventional sintering because of conductive and radioactive heat tr...