Preparation of superionic ceramics by spark plasma method

Microstructure of spark plasma sintered TiB2 and TiB2–AlN ceramics

In this research study, the effects of aluminum nitride (AlN) additive on the densification behavior and microstructure development of titanium diboride (TiB2) based ceramic matrix composite were investigated. In this way, a monolithic TiB2 ceramic and a TiB2–5 wt% AlN ultrahigh temperature ceramic composite were fabricated by spark plasma sintering (SPS) proces...

Optically transparent ceramics by spark plasma sintering of oxide nanoparticles

Comparison of Creep Behavior in Alumina Based Ceramics Densified by Spark Plasma Sintering and Hot Pressing

Spark plasma sintering (SPS) method, as plasma activated sintering, is a method applicable for rapid sintering of metals and ceramics. Owing to the advantage of rapid heating, the alumina ceramics obtained by SPS have a grain size and density comparable to those of hot pressed ones. The increase of densification rate may be related to some difference in ion transport characteristics. This study...

Preparation of phase pure, dense fine grained ceramics by conventional and spark plasma sintering of La-substituted BiFeO3 nanoparticles

High density ceramics of the system Bi1-xLaxFeO3, 0 ≤ x ≤ 0.15, have been prepared starting from nanoparticles obtained by mechanosynthesis. The ceramics have been sintered conventionally at 850oC and by spark plasma sintering (SPS). Sintering conditions have been optimized to obtain single phase ceramics, and the microstructure of the ceramics has been compared. Ceramics prepared conventionall...

Microstructure and Properties of Spark Plasma Sintered MoAlB Ceramics

Advisor: Bai Cui Molybdenum aluminum boride (MoAlB) is a ternary transition metal boride which has promising aeronautic and nuclear applications. It inheres excellent properties of the binary transitional metal borides (e.g., MoB, ZrB2) such as high melting temperature, high hardness, and thermal conductivity. Besides, MoAlB is superior to MoB because: (1) the Al element provides an oxidation r...