Restraints on backbone conformations in solid state NMR studies of uniformly labeled proteins from quantitative amide 15N–15N and carbonyl 13C–13C dipolar recoupling data
نویسندگان
چکیده
منابع مشابه
Multidimensional dipolar exchange-assisted recoupling measurements in solid-state NMR.
Aseries of uni- and multidimensional variants of the dipolar exchange-assisted recoupling (DEAR) NMR experiment is described and applied to determinations of (13)C-(14)N dipolar local field spectra in amino acids and dipeptides. The DEAR protocol recouples nearby nuclei by relying on differences in their relative rates of longitudinal relaxation, and has the potential to give quantitative geome...
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ژورنال
عنوان ژورنال: Journal of Magnetic Resonance
سال: 2012
ISSN: 1090-7807
DOI: 10.1016/j.jmr.2012.03.001