Simultaneous determination of Pb and Cd in seafood by ICP OES with on-line pre-concentration by solid phase extraction with amberlite XAD-4 after complex formation with DDTP

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Determination of some trace metals by FAAS after solid-phase extraction with amberlite XAD-1180/TAN chelating resin.

A new chelating resin was synthesized by immobilizing 1-(2-thiazolylazo)-2-naphthol through the -N=N- group on Amberlite XAD-1180. The resin was used for the preconcentration of Cd(II), Co(II), Cu(II), Mn(II), Ni(II), and Pb(II) ions and their determination by flame atomic absorption spectrometry (FAAS). The influences of some analytical parameters, such as the pH, volume of the sample, flow ra...

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Nickel determination in saline matrices by ICP-AES after sorption on Amberlite XAD-2 loaded with PAN.

In the present paper, a solid phase extraction system for separation and preconcentration of nickel (ng g(-1)) in saline matrices is proposed. It is based on the adsorption of nickel(II) ions onto an Amberlite XAD-2 resin loaded with 1-(2-pyridylazo)-2-naphthol (PAN) reagent. Parameters such as the pH effect on the nickel extraction, the effect of flow rate and sample volume on the extraction, ...

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ژورنال

عنوان ژورنال: Brazilian Archives of Biology and Technology

سال: 2013

ISSN: 1516-8913

DOI: 10.1590/s1516-89132013000100017