Synthesis and Molecular Structure of [Ru 3 (CO) 10 (μ‐dppa)] (dppa = Ph 2 PN(H)PPh 2 ) Provided by Its Dioxane Solvate
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Crystal structure of AI ( tBu ) 3 ( NH 2 CH 2 CH 2 Ph ) : A molecular " slinky "
The molecular structure of AI(tBu)3(NH2CH2CHzPh) is determined by the crystal packing of the phenyl rings and the pseudo spherical Al(tBu)3 units, and may be viewed as a layered structure consisting of double sheets of the phenyl rings and the Al(tBu)3 units. The A1-N-C-C linkage shows severe disorder as a result of its flexibility. The structure of Al(tBu)3 (NH2CH2CH2Ph) can be likened to a mo...
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A 3-hydro-4-pyridinone compound derived from maltol and dopamine has been prepared using a microwave reactor. The molecular structure of the protonated product was confirmed by single crystal X-ray diffraction. Crystals were obtained from a saturated solution of methanol and belong to the triclinic space group P-1 with unit cell parameters a = 8.3801(11) Å; b = 9.2583(12) Å; c = 11.5671(15) Å; ...
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2-Benzylaminopyridine (HBAP) reacts with NaH in THF and generates the sodium salt (NaBAP). Further reaction of [Cu(TMEDA) ] [CuCl ] with one equivalent of this ligand in THF leads to the formation of a dimeric Cu(1) complex, [Cu (BAP)] . H 0. The molecular structure has been determined by using a single-crystal X-ray diffraction method. The yellow compound crystallizes in the monoclinic s...
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The crystal structure of the title Schiff base complex is obtained by single-crystal X-ray diffraction data.The solid state structure determination reveals that the coordination geometry around the copper(II) center istetrahedrally distorted square-planar. The crystal packing shows one dimensional infinite chains which arisesfrom the intermolecular interaction and stabilize the crystal packing.
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Departamento de Fı́sica, Facultad de Bioquı́mica y Ciencias Biológicas, Universidad Nacional del Litoral and INTEC (CONICET-UNL), Güemes 3450, 3000 Santa Fe, Argentina, Departamento de Fı́sica, Comisión Nacional de Energı́a Atómica, Avda. del Libertador 8250, 1429 Buenos Aires, Argentina, Departamento de Fı́sica, Facultad de Ciencias Fı́sicas y Matemáticas, Universidad de Chile, Avda. Blanco Encalada...
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ژورنال
عنوان ژورنال: Zeitschrift für anorganische und allgemeine Chemie
سال: 2020
ISSN: 0044-2313,1521-3749
DOI: 10.1002/zaac.202000359