Synthesis of MgB2 at Low Temperature and Autogenous Pressure

Synthesis of MgB2 at Low Temperature and Autogenous Pressure

High quality, micron-sized interpenetrating grains of MgB₂, with high density, are produced at low temperatures (~420 °C < T < ~500 °C) under autogenous pressure by pre-mixing Mg powder and NaBH₄ and heating in an Inconel 601 alloy reactor for 5-15 h. Optimum production of MgB₂, with yields greater than 75%, occurs for autogenous pressure in the range 1.0 MPa to 2.0 MPa, with the reactor at ~50...

Diamond synthesis from carbon nanofibers at low temperature and low pressure

In this article, we report a new route to synthesize diamond by converting "solid" carbon nanofibers with a Spark Plasma Sintering system under low temperature and pressure (even at atmospheric pressure). Well-crystallized diamond crystals are obtained at the tips of the carbon nanofibers after sintering at 1500 °C and atmospheric pressure. Combining with scanning electron microscopy, transmiss...

Low-temperature olivine rheology at high pressure

San-Carlos olivine rheology was investigated at pressure (P) up to 9 GPa and temperature (T) lower than 890 ◦C. Six powder specimens were cold compressed and sintered into dense and compact materials, then deformed during relaxation experiments carried out at constant pressure and temperature in DIA-type cubic-anvil apparatus. Sample elastic strain was monitored during relaxation by in situ X-r...

Synthesis of coesite nanocrystals from ethane bridged periodic mesoporous organosilica at low temperature and extreme pressure.

Coesite nanocrystals have been synthesized from periodic mesoporous organosilica (PMO) with (CH(2))(2) bridges heated at 300 °C for 150 min and 12 GPa. The crystals are not sintered, single crystalline, and have diameters of ca. 100-300 nm. Below 300 °C, an amorphous non-porous organosilica glass was obtained. Heating above 300 °C at 12 GPa results in the rapid crystal growth and micron size co...

Lyophilizing Foot-and Mouth Disease Virus at Low Drying Temperature