Synthesis of N, N΄3, 4-Dialkylamino-1, 2, 5-Oxadiazoles
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Abstract:
N, N΄-3, 4-di(methylamino)-1, 2, 5-oxadiazole (1f) was prepared by dehydration of N, N΄-3, 4-di(methylamino)glyoxime (2f) in aqueous potassium hydroxid at 170-180 ˚C. Under similar conditions N, N΄-3, 4-di(benzylamino)-1, 2, 5-oxadiazole (1c) and N, N΄-3, 4-di(isopropylamino)-1, 2, 5-oxadiazole (1e) were not obtained, but, N, N΄-3, 4-di(ethylamino)-1, 2, 5-oxadiazole (1g) was appeared with small amount.
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Journal title
volume 22 issue 2
pages 13- 15
publication date 2003-12-01
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