Preparation and Characterisation of ZnO - SiO2 and Bi2O3 – CuO Nanocomposites

نویسندگان

  • Thambu Sornakumar Department of Mechanical Engineering, Thiagarajar College of Engineering Madurai 625006, T.N., India
چکیده مقاله:

In the present work, ZnO - SiO2 and Bi2O3– CuO nanocomposites have been prepared by sol gel with alternate precursors existing in literature. They are characterised by XRD, SEM,UV, FTIR and photoluminescence  spectra .The XRD results indicate a crystallite size of  approximately 80 nm for both nanocomposites. SEM image shows a heterogeneous particle size for both samples. The band gap of ZnO - SiO2 and Bi2O3– CuO obtained from Taucs plot is 4.1 eV and 2.85 eV, respectively. PL spectra show high intensity absorption for ZnO-SiO2 in comparison to   Bi2O3–CuO. The composites of Bi2O3–CuO is recommended for efficient optical coating against the coating made from Bi2O3.

برای دانلود باید عضویت طلایی داشته باشید

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

Preparation, characterization and determination of photocatalytic activity of MCM-41/ZnO and MCM-48/ZnO nanocomposites

The direct and indirect methods in solvent media and grinding method in a solvent-free media were used to prepare the MCM-41/ZnO and MCM-48/ZnO photocatalysts. The X-ray diffraction (XRD) patterns showed that zinc oxide nanoparticles were put into MCM-41 and MCM-48 substrates and there were ZnO crystallites as secondary phase in the extra framework of mesoporous materials. The decrease of surfa...

متن کامل

Preparation, characterization and determination of photocatalytic activity of MCM-41/ZnO and MCM-48/ZnO nanocomposites

The direct and indirect methods in solvent media and grinding method in a solvent-free media were used to prepare the MCM-41/ZnO and MCM-48/ZnO photocatalysts. The X-ray diffraction (XRD) patterns showed that zinc oxide nanoparticles were put into MCM-41 and MCM-48 substrates and there were ZnO crystallites as secondary phase in the extra framework of mesoporous materials. The decrease of surfa...

متن کامل

Linear and nonlinear optical characteristics of ZnO-SiO2 nanocomposites.

We present the spectral and nonlinear optical properties of ZnO-SiO2 nanocomposites prepared by colloidal chemical synthesis. Obvious enhancement of ultraviolet (UV) emission of the samples is observed, and the strongest UV emission of a typical ZnO-SiO2 nanocomposite is over three times stronger than that of pure ZnO. The nonlinearity of the silica colloid is low, and its nonlinear response ca...

متن کامل

Preparation and Characterization of ZnO Nanoparticles Supported on Amorphous SiO2

In order to reduce the primary particle size of zinc oxide (ZnO) and eliminate the agglomeration phenomenon to form a monodisperse state, Zn2+ was loaded on the surface of amorphous silica (SiO₂) by the hydrogen bond association between hydroxyl groups in the hydrothermal process. After calcining the precursors, dehydration condensation among hydroxyl groups occurred and ZnO nanoparticles suppo...

متن کامل

Study of structural, optical and electrical properties of ZnO/CuO nanocomposites

In this work, the first ZnO/CuO nanocomposites were synthesized by chemical vapour deposition (CVD), thermal evaporation (PVD) and sputtering on silicon substrates (Si). Then, the structural, optical and electrical properties of the samples were investigated. Examination of the X-ray diffraction patterns confirmed the mixed-phase formation of hexagonal zinc oxide (ZnO) and monoclinic copper oxi...

متن کامل

Sol-gel Synthesis of ZnO Nanoparticles and ZnO-TiO2-SiO2 Nanocomposites and Their Photo-catalyst Investigation in Methylene Blue Degradation

In this work firstly ZnO nanoparticles were synthesized via a simple precipitation method. At the second step titanium dioxide and silicon dioxide shell were synthesized on the core. For preparation ZnO-TiO2-SiO2 the sol product was calcinated at 500 ºC for 2h. Properties of the product were examined by X-raydiffraction pattern (XRD), scanning electron microscope (SEM) and Fourier transform inf...

متن کامل

منابع من

با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

ذخیره در منابع من قبلا به منابع من ذحیره شده

{@ msg_add @}


عنوان ژورنال

دوره 3  شماره 1

صفحات  79- 84

تاریخ انتشار 2018-01-01

با دنبال کردن یک ژورنال هنگامی که شماره جدید این ژورنال منتشر می شود به شما از طریق ایمیل اطلاع داده می شود.

کلمات کلیدی

میزبانی شده توسط پلتفرم ابری doprax.com

copyright © 2015-2023