نتایج جستجو برای: combustion synthesis

تعداد نتایج: 438403  

Boron carbide is one of the hardest materials. The combustion method was used to synthesize B4C-TiB2 nanocomposite powder in a B2O3-Mg-TiO2-C system. An experimental study of the formation of B4C–TiB2 nanoparticles was conducted in the thermal explosion mode. A mixture of B2O3:TiO2:Mg:C at a molecular ratio of 3:1:12:1 was chosen to obtain the B4C–TiB2. This powder mixture was milled for differ...

Nanocomposite of titanium diboride/titanium carbide was fabricated by combustion synthesis of mechanically milled reactant powders. The stoichiometric mixture of Ti and B4C as starting materials milled for 1, 3, 6 and 9 h. Milled powders pressed to form pellets then green compacts were placed in a tube furnace that preheated to 1100 oC in inert atmosphere (Ar).The samples were investigated by X...

پایان نامه :وزارت علوم، تحقیقات و فناوری - دانشگاه رازی - دانشکده علوم 1390

in this thesis, a better reaction conditions for the synthesis of spirobarbiturates catalyzed by task-specific ionic liquid (2-hydroxy-n-(2-hydroxyethyl)-n,n-dimethylethanaminium formate), calcium hypochlorite ca(ocl)2 or n-bromosuccinimide (nbs) in the presence of water at room temperature by ultrasonic technique is provided. the design and synthesis of spirocycles is a challenging task becaus...

M. Farahmandjou N. Golabiyan

The aluminum oxide materials are widely used in ceramics, refractories and abrasives due to their hardness, chemical inertness, high melting point, non-volatility and resistance to oxidation and corrosion. The paper describes work done on synthesis of α-alumina by using the simple, non-expensive solution combustion method using glycine as fuel.Aluminum oxide (Al2O3) nanoparticles were synthesiz...

CrN/Cu composite powders were synthesized by employing a novel two-step technique. Firstly, the Cr2O3+CuO precursors were prepared by the solution combustion synthesis (SCS) method using cupric nitrate, urea, and chromium nitrate as initial materials. Subsequently, the SCS precursors were calcined at 850 °C in NH3 for 6 h, and transformed to CrN/Cu composite powders. The composite powders consi...

Journal: :Chemical communications 2012
Zhaoyang Fei Shengchao He Lei Li Weijie Ji Chak-Tong Au

We reported the morphology-directed synthesis of Co(3)O(4) nanotubes via interfacial reaction of NaOH with pre-fabricated CoC(2)O(4)·2H(2)O nanorods based on modified Kirkendall effect. The as-obtained Co(3)O(4) nanotubes showed excellent activity and durability in catalytic combustion of CH(4).

2006
S. D. Bakrania C. Perez M. S. Wooldridge

Combustion synthesis of tin dioxide (SnO2) was studied using a new synthesis approach where the combustion environment was augmented to control the temperature and flow conditions using methane as a supplemental fuel. The experiments were carried out at atmospheric pressure using a multi-element diffusion flame burner with a gas-phase precursor for SnO2 and solid-phase precursor for metal addit...

A. Said and M.A. Golozar,

Combustion synthesis has been used to produce Fe-(Ti,W)C composites. A simple reactor was designed which made it possible to ignite the samples under controlled atmosphere. Samples with different W/Ti ratio were ingnited under argon atmosphere by an electric arc and a self-propagating reaction was initiated in each sample. Different composites such as WC in Fe-Ti matrix, WC+(Ti,W)C in Fe matrix...

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