نتایج جستجو برای: x ray diffraction and ftir

تعداد نتایج: 16938614  

Journal: :international journal of nano dimension 0
k. tahvildari department of chemistry, islamic azad university, north tehran branch, tehran, iran. m. esmaeili pour department of chemistry, islamic azad university, north tehran branch, tehran, iran. sh. ghammamy department of chemistry, islamic azad university, takestan branch, takesatn, iran. h. nabipour department of chemistry, islamic azad university, takestan branch, takesatn, iran.

the aim of the present study was to prepare nano-sized calcium fluoride (caf2). calcium fluoride nanoparticles were synthesized by cacl2.6h2o and ammonium fluoride. nanoparticles were synthesized by co-precipitation method. the synthesized nanocrystals were characterized by x-ray diffraction (xrd), fourier transform infrared spectroscopy (ftir), scanning electron microscopy (sem). the crystalli...

Hydroxyapatite nanorods aligned with ultrahigh crystallinity and high-yield were successfully synthesized through a hydrothermal approach. In this experiment, a new composition of cetyltrimethylammonium bromide ((CH3(CH2)15N+(CH3)3Br-) was designated as CTAP)/Ca(NO3)2/(NH4)2HPO4/NaOH and distilled water under hydrothermal condition, to synthesize single crystalHAp nanorods with diameter of 20 ±...

Biological synthesis of metallic nanoparticles is considered as a fast, eco-friendly, affordable and easily scalable technology. Also, the nanoparticles produced by plants are very stable. In this study, the focus is on the synthesis of silver nanoparticles using extract of eryngium campestre. The effective parameters such as concentration of silver nitrate, pH, temperature and time, size and m...

In recent years, green synthesis of nanoparticles has attracted a great attention because of medicine and biological applications. In this work, bismuth oxide nanoparticles (Bi2O3 NP) was prepared via green synthesis using mentha pulegium aqueous extract after 24 h at 90°C. The product was characterized by ultraviolet-visible (UV-VIS) spectrophotometer, Fourier transform infrared (FTIR), X-ray ...

In this study, the main objective is the preparation and the characterization of a modified Algerian bentonite based adsorbent by intercalation with hexadecyltrimethylammonium bromide (HDTMA). Natural and modified bentonites were characterized using thermogravimetric analysis (TGA), X-ray diffraction (XRD) and infrared spectroscopy (FTIR). The X-ray results indicate that the geometry of the int...

In this paper, undopedZnO and Co-ZnOnano structureswith different molar ratio of Cobalt have been synthesized by the sonochemical method. Structure have been characterized by Fourier Transform (FTIR) and UV–Vis spectroscopy,Scanning Electron Microscopy (SEM), Energy Dispersive Analytical X-Ray (EDAX), and X-Ray Diffraction (XRD) methods. Moreover, the direct band gap has been calculated by Tauc...

2017
Daniela Predoi Simona Liliana Iconaru Aurélien Deniaud Mireille Chevallet Isabelle Michaud-Soret Nicolas Buton Alina Mihaela Prodan

The present work was focused on the synthesis and characterization of hydroxyapatite doped with low concentrations of zinc (Zn:HAp) (0.01 < xZn < 0.05). The incorporation of low concentrations of Zn2+ ions in the hydroxyapatite (HAp) structure was achieved by co-precipitation method. The physico-chemical properties of the samples were characterized by X-ray Diffraction (XRD), Fourier Transform ...

In this paper, undopedZnO and Co-ZnOnano structureswith different molar ratio of Cobalt have been synthesized by the sonochemical method. Structure have been characterized by Fourier Transform (FTIR) and UV–Vis spectroscopy,Scanning Electron Microscopy (SEM), Energy Dispersive Analytical X-Ray (EDAX), and X-Ray Diffraction (XRD) methods. Moreover, the direct band gap has been calculated by Tauc...

The purpose of the present study was to synthesize and characterize nanosilica from alkali-extraction of silica fume under controlled conditions using poly (vinyl alcohol) (PVA) as a dispersing agent. The dissolution efficiency of silica fume was affected by various factors such as concentration of the reagent, reaction time and temperature. A maximum dissolution efficiency of 91% was achieved ...

Co@pyr/APTZCMNPs was synthesized, and some of its characteristic analyses, such as Fourier transform infrared spectroscopy (FTIR), thermogravimetric analysis (TGA), scanning electron microscopy (SEM), energy dispersive X-ray (EDX) and X-ray diffraction (XRD) were investigated. The results indicated that this heterogeneous catalyst was an excellent and reusable system to synthesize of 14H</e...

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