This work shows the benefits of characterizing historic paintings via compositional and microtextural data from micro-X-ray diffraction (μ-XRD) combined with molecular information acquired with Raman microscopy (RM) along depth profiles in paint stratigraphies. The novel approach was applied to identify inorganic and organic components from paintings placed at the 14th century Islamic Universit...

the x-ray charge density analysis of a hydroxynaphthoquinnne derivative was obtained by multipolar hansen-coppens formalism refinement through high resolution x-ray diffraction data at 100(1) k. the molecularproperties of the title compound resulted from the combined experimental and the quantum theory of atoms inmolecules (qtaim) studies. the topological properties of the covalent bonds and of...

the knoevenagel condensation of aromatic aldehydes with barbituric acid, dimedone and malononitrile occurred in the presence of bf3/nano-γ-al2o3 at room temperature in ethanol. this catalyst is characterized by powder x-ray diffraction (xrd), fourier transform infrared spectroscopy (ft-ir), thermal gravimetric analysis (tga), field emission scanning electron microscopy (fesem) and energy-disper...

Abstract: Austenitic stainless steels exhibit a low hardness and weak tribological properties. The wear behaviour of austenitic stainless steel AISI 316 was evaluated through the pin on disc tribological method. For investigating the effect of wear on the changes in microstructure and resistance to wear, optical microscopy and scanning electron microscope were used. The hardness of the worn...

Several studies have shown that macro micro porous bioceramics ectopically implanted promote bone tissue formation. This study aims at investigating the inflammatory response towards biphasic calcium phosphate (BCP) ceramic micro particles. BCP composed of hydroxyapatite (HA) and beta-tricalcium phosphate, HA/beta -TCP ratio of 50/50, were prepared by sintering at 1200 degrees C for 5 h. After ...

Hydroxyapatite (HA) is the most important bioactive ceramics because of biocompatibility and structural similarity to the mineral part of bones and teeth of broad clinical application in the field of dentistry, orthopedic and coatings are Biomaterials. The aim of this study was to construct nano-hydroxyapatite micro particles using calcite, silica and zinc oxide using ball milling, powder, thes...

In this paper we discuss a choice between the diffractive and refractive binary micro-lenses for the longwave IR FPA. To investigate diffraction on the micro-lenses we have used a numerical code based-on the rigorous electromagnetic theory, because neither geometrical optics nor thin element approach of scalar diffraction theory can correctly describe waveguide, shadowing and interference effec...

the structure of the nonaaquayttrium (iii) bromate, [y(h2o)9](bro3)3, at low temperature (100 k) has been studied by means of single-crystal x-ray diffraction. crystallography shows a hexagonal unit cell, space group p63/mmc (no. 194) with z = 2, a = b = 11.7104(11) å, c = 6.6259(5) å and v = 786.90(12) å3 at 100 k. the hydrated trivalent yttrium(iii) ion forms a tricapped trigonal prism, in wh...

in this research calcium fluoride nanoparticles and its different amount of cerium ion dopant (5%and 10%) were prepared. the mentioned nanoparticle were studied by fourier transform infrared spectroscopy (ftir) , x-ray diffraction (xrd), absorption and photoluminescence spectra (pl) and scanning electron microscopy (sem). the xrd patterns indicate a typical cubic fluorite structure and no other...

x-ray diffraction peak profile analysis was used to identify changes in the lattice distortions during isothermal aging of fe-10ni-7mn (wt. %) maraging steel. integral peak breadths were analyzed using classical williamson-hall equation taking the elastic anisotropy into account. it was found that substantial lattice distortions rise during precipitation hardening which depend strongly on the s...