Alumina gels were prepared by the sol–gel method using alumatrane or tris(alumatranyloxy-i-propyl)amine as precursor synthesised directly from the reaction of inexpensive and readily available compounds, aluminium hydroxide and triisopropanolamine (TIS), via the one step process. Sol–gel process parameters, such as gel time, were correlated to variables of the initial stage of the process, such...

Ta2O5 nanoparticles have been synthesized from alkoxy carboxylates of tantalum via the sol-gel route. Tantalum alkoxides were reacted with chlorocarboxylic acids in order to lower the susceptibility hydrolysis. When these modified alkoxy carboxylates were used in the sol-gel synthesis, they yielded Ta2O5 nanoparticles of better properties than those of the alkoxide-derived Ta2O5 nanoparticles. ...

tio2/magnetit and tio2/nd/magnetit were prepared and used for photocatalytic decomposition of the methylorange as a pollutant. tio2 and tio2/nd were prepared by sol gel method and were characterized using xrd, ft ir and tem. the prepared catalysts were deposited on magnetite surface to have a catalyst with magnetite core. so the catalyst can be separated easily from the waste solution by a magn...

zinc oxide (zno) nanopowders were synthesized by the sol–gel method from an ethanol solution of zinc sulfate heptahydrate in the presence of diethylene glycol surfactant. detailed structural and microstructural investigations were carried out using x-ray diffraction (xrd), high-resolution transmission electron microscopy (hrtem), field emission scanning electron microscopy (fe-sem), fourier tra...

mntio3-zeolite-y nanocomposites were synthesized with 5-10-20% (w/w) of mntio3 by stearic acid gel method. then, the gels were calcined at 900 °c for 4 hours and the resulted spectra were investigated at 20% (w/w) concentration. also, the presence of rhombohedral phase of mntio3 in zeolite-y matrix was confirmed by xrd, sem, edx and bet. the vsm results showed the antiferromagnetic properties f...

highly sinterable alumina nano-powders have been synthesized by a sol-gel combustion method with glycine asfuel. the preparation involved the thermal decomposition of a chelating agent (fuel)-nitrate gel and theformation of amorphous precursors. the nanopowders calcined at 1100°c were characterized by x-ray powderdiffraction (xrd) and scanning electron microscopy (sem). it was found that the ch...

various concentrations of copper were embedded into silica matrix to xerogel forms using copper source cu(no3)2∙3h2o. the xerogel samples were prepared by hydrolysis and condensation of tetraethyl ortho-silicate (teos) with determination of new molar ratio of the components by the sol-gel method. after ambient drying, the xerogel samples were heated from 60 to 1000˚c at a slow heating rate (50°...

in this study, sio2 nanoparticles were successfully synthesized via sol-gel precipitation method and the effects of different parameters such as temperature, ethanol, ammonia and tetraethylorthosilicate (teos) contents based on water were investigated in a systematic way applying taguchi experimental design method. it was found that, among all the investigated parameters, ethanol as a co-solven...