This method for determining aluminum in human serum involves electrothermal atomic absorption spectrophotometry. A longer drying time allows less pre-dilution of the sample, and the method also includes a flush cycle after atomization. Standard-addition methodology is used to eliminate matrix effects and the need for a standard curve. We used this method on serum from 50 normal persons and from...

Early detection of non blanching erythema (pressure ulcer category I) is necessary to prevent any further skin damage. An objective method to discriminate between blanching/non blanching erythema is presently not available. The purpose of this investigation was to explore if a non invasive objective method could differentiate between blanching/non blanching erythema in the sacral area of patien...

PURPOSE Analysis of drugs in multicomponent system officially is carried out using chromatographic technique, however, this technique is too laborious and involving sophisticated instrument. Therefore, UV-VIS spectrophotometry coupled with multivariate calibration of partial least square (PLS) for quantitative analysis of metamizole, thiamin and pyridoxin is developed in the presence of cyanoco...

A method has been described for the estimation of calcium and magnesium in serum and urine using atomic absorption spectrophotometry. The precision and accuracy of the techniques have been determined and were found to be acceptable. THE RANGE OF VALUES FOR CALCIUM AND MAGNESIUM IN THE SERA OF NORMAL ADULTS WAS FOUND TO BE: serum calcium (corrected to a specific gravity of 1.026) 8.38-10.08 mg. ...

BACKGROUND Estimation of the quantity of colostral IgG or serum IgG absorbed following ingestion of colostrum by calves is essential for monitoring the effectiveness of colostrum feeding practices on dairy farms. Milk total solids concentrations determination is a critical part of quality assessment of nonsaleable whole milk prior to feeding to calves. To date, on-farm methods to assess colostr...

In this study, the trace amounts of erythrosine, as a food dye is determined by cloud point extraction-scanometry (CPE-Scanometry) as a new, facile, available, fast, sensitive, and low cost method. The method is based on the CPE of analyte from aqueous solution, diluting the extracted surfactant-rich phase with ethanol, transfer to Plexiglas®cell and scanning the cells containing the...

A micell-mediated phase separation method for preconcentration of ultra-trace quantities of mercury as a prior step to its determination by UV-Vis spectrophotometry has been developed. The method is based on Hg(II)-dithizone complex formation in alkaline aqueous solution, and extraction of this Hg(II)-dithizone secondary complex into the surfactant-rich phase of the non-ionic surfactant oct...

Three sensitive, selective and reproducible stability-indicating methods are presented for determination of nitazoxanide (NTZ), a new anti-protozoal drug, in presence of its degradation products. Method A utilizes the first derivative of ratio spectra spectrophotometry by measurement of the amplitude at 364.4 nm using one of the degradation products as a divisor. Method B is a chemometric-assis...

The objective o f this study was to develop simple and rapid method for the determination of ciprofloxacin hydrochloride in ophthalmic solution using UV spectrophotometry. The intrinsic absorbance of ciprofloxacin was measured directly at 275 nm. The calib ration graph was linear over the range 2.0–7.0 μg mL with relative standard deviations (RSD) values ranging from 1.55 to 2.47% (n=6). The me...