Nanoporous silicon powder was produced via efficient magnesiothermic reduction. In this work, the thermal effect and reduction process time were investigated on the porous silicon structure. The nanoporous silicon powders were characterized by  X-ray diffraction analysis and field emission scanning electron microscopy. The results demonstrate that porous structure was changed to homogeneous and...

To develop an effective process for tantalum powder production, a new preform reduction process (PRP) based on the magnesiothermic reduction of feed preform containing tantalum oxide (Ta2O5) was investigated. The feed preformwas fabricated from slurry, which was made by mixing Ta2O5 powder, flux (e.g., CaCl2), and binder. Various compositions of preform in the form of plates were prepared using...

The influence of magnesium content on the mechanosynthesis of ZrB2–SiC–ZrC composite in Mg/ZrSiO4/B2O3/C mixture was investigated. Thermodynamic evaluations revealed that the amount of Mg played a main role, thereby; the overall reaction enthalpy and adiabatic temperature (Tad) changed by variation of magnesium content. According to differential thermal analysis (DTA) results, after 45min milli...

Herein, porous nano-silicon has been synthesized via a highly scalable heat scavenger-assisted magnesiothermic reduction of beach sand. This environmentally benign, highly abundant, and low cost SiO₂ source allows for production of nano-silicon at the industry level with excellent electrochemical performance as an anode material for Li-ion batteries. The addition of NaCl, as an effective heat s...

Highly monodisperse porous silicon nanospheres (MPSSs) are synthesized via a simple and scalable hydrolysis process with subsequent surface-protected magnesiothermic reduction. The spherical nature of the MPSSs allows for a homogenous stress-strain distribution within the structure during lithiation and delithiation, which dramatically improves the electrochemical stability. To fully extract th...

Lithium-ion batteries (LIBs) have been one of the most predominant rechargeable power sources due to their high energy/power density and long cycle life. As promising candidates for new generation negative electrode materials in LIBs, silicon has advantages specific capacity, a lithiation potential range close that lithium deposition, rich abundance earth’s crust. However, commercial use LIBs i...