A variety of iron(iii) oxides and oxyhydroxides were synthesised and characterised using three distinct methods of preparation: microemulsion, precipitation and sol-gel. The results clearly showed that the structure, textural properties, crystal morphology and catalytic performance of the phases obtained were highly dependent on the chemical routes used for the synthesis. Precipitation and micr...

Hydroxyapatite (HAP) ceramics belongs to a class of calcium phosphate-based biomaterial, which has been widely used as bone substitute for long time. In recent years, synthetic HAP has assumed substantial interest and importance due to its chemical similarity with the natural Ca phosphate mineral present in a biological hard tissue. Considering the wide applications of calcium phosphate compoun...

Abstract Different alumina samples prepared with sol–gel, chemical precipitation and hydrothermal synthesis were used as supports of Fe-promoted Rh-based catalysts for ethanol via CO hydrogenation. The characterized by means N 2 -adsorpotion, XRD, H -TPR, XPS, STEM, -TPD, DRIFTS, chemisorption. results indicated that the Al O 3 exhibited nano-fiber morphology constituted mixed crystal phases, w...

Bioactive glass with composition SiO2, Na2O, CaO, P2O5 with MgO additive were synthesized through a quick alkali mediated sol–gel method. MgO was substituted for SiO2 in glass formula up to 5 wt% and in-vitro bioactivity of the samples (precipitation behavior of carbonated apatite likely bone layer) was evaluated by soaking them in simulated body fluid (SBF). The characterizations were carried ...

Novel hybrid xerogel materials were synthesized by a sol-gel procedure. n-octadecyltriethoxysilane was co-condensed with and without different cross-linkers using Q(0) and T(0) mono-functionalized organosilanes in the presence of n-hexadecylamine with different hydroxyl silica functional groups at the surface. These polymer networks have shown new properties, for example, a high degree of cross...

Mn-based catalysts enable high NO x conversion in the selective catalytic reduction of NO x with NH3. Three catalyst-production methods, namely, co-precipitation, impregnation, and sol-gel, were used in this study to determine the optimum method and parameters. The maximum catalytic activity was found for the catalyst prepared by sol-gel with a 0.5 Mn/Ti ratio. The denitrification efficiency us...

In this paper, indium tin oxide (ITO) nanoparticles has been prepared by chemical methods under given conditions with solution of indium chloride (InCl3·4H2O), tin chloride (SnCl4·5H2O) in ammonia solution. The samples were characterized by X-ray Diffraction (XRD) and scanning electron microscopy (SEM) analyses after heat treatments. The SEM results showed that, the size of the ITO particles pr...

High surface area ceria nanoparticles have been prepared using a citrate sol-gel precipitation method. Changes to the particle size have been made by doping ceria powders, and calcining at different temperatures. Xray methods were used to determine their lattice parameters. The particle sizes have been assessed using transmission electron microscopy (TEM) and the lattice parameter found to fall...