In this study, the commercial TiO2 nanopowder and micropowder of anatase phase and rutile phase have been characterized by x-ray diffraction (XRD) and transmission electron microscopy (TEM). XRD patterns of nano-TiO2 in rutile and anatase phases exhibit broad peaks whereas both phases of micro-TiO2 demonstrate very sharp peaks. TEM images show that the grain size of TiO2 micropowders and TiO2 n...

      In this research, TiO2 nanoparticles were synthesized by a simple wet chemical method. TiCl4 was used as precursor in hydrogen peroxideand ethanol. The TiO2 nanoparticles were characterized by transmission electron microscopy (TEM), scanning electron microscopy (SEM), X-ray diffraction (XRD), electron dispersive spectroscopy (EDS) and UV-Vis spectrophotome...

The isothermal section of the Ce-Mg-Zn system at 300 °C was experimentally established in the full composition range via diffusion multiple/couples and key alloys. Annealed key alloys were used to confirm the phase equilibria obtained by diffusion multiple/couples and to determine the solid solubility ranges. Spot analysis was carried out, using wavelength dispersive X-ray spectroscopy (WDS), t...

we report on the synthesis, morphology, chemically and structurally of tio2-cuo-sio2 nanostructure with different precursors molar ratio and calcined temperatures. in the present work, ternary reactive powders in the tio2-cuo-sio2 systems have been obtained using the sol-gel method, by the simultaneous gelation of all cations. the compounds and other elements change in special chemical and phys...

The MgB2 bulks were prepared by high energy milling of Mg and B powder. The correlations among milling times, microstructure and superconducting properties were investigated in MgB2 bulks. Samples were characterized by x-ray diffraction (XRD), energy dispersive spectrometry (EDX) and scanning electron microscope (SEM), and the magnetization properties were examined by a Superconducting quantum ...

In this work, nanostructured Mg-Al-Nd alloys were successfully fabricated using mechanical alloying method. Phase structures of the milled powders and the extruded rods were examined using X-ray diffraction (XRD) and the microstructures were observed using a transmission electron microscope (TEM). The element distributions were also examined by an energy dispersive spectroscopy (EDS) system. Th...

Magnesium is potentially useful for orthopedic and cardiovascular applications. Magnesium and its alloys are light, biodegradable, biocompatible metals that have promising applications as biomaterials. However, the corrosion rate of this metal is so high that its degradation occurs before the end of the healing process. One of the ways to improve the corrosion rate is to compose it with ceramic...

Magnesium is potentially useful for orthopedic and cardiovascular applications. Magnesium and its alloys are light, biodegradable, biocompatible metals that have promising applications as biomaterials. However, the corrosion rate of this metal is so high that its degradation occurs before the end of the healing process. One of the ways to improve the corrosion rate is to compose it with ceramic...

The morphology and structure of 2,2':6',2″-ternaphthalene (NNN) deposited on muscovite mica(001) substrates was investigated by scanning force microscopy (SFM) and specular X-ray diffraction measurements. Consistently, both methods reveal the coexistence of needle-like structures with a {111} contact plane and {001} orientated island-like crystallites, which are built up by almost upright stand...

In this study, a simple, rapid, and eco-friendly green method was introduced to synthesize magnetite nanoparticles (Fe3O4-NPs) successfully. Seaweed Kappaphycus alvarezii (K. alvarezii) was employed as a green reducing and stabilizing agents. The synthesized Fe3O4-NPs were characterized with X-ray diffraction (XRD), ultraviolet-visible spectroscopy (UV-Vis), Fourier transform infrared (FT-IR), ...