The Si-coated SiC (Si-SiC) composite nanoparticle was prepared by non-transferred arc thermal plasma processing of solid-state synthesized SiC powder and was used as a sintering additive for SiC ceramic formation. Sintered SiC pellet was prepared by spark plasma sintering (SPS) process, and the effect of nano-sized Si-SiC composite particles on the sintering behavior of micron-sized SiC powder ...

TaC and HfC are thought to have the highest melting point (~4000°C) among all refractory materials. The binary solid solution of TaC and HfC (Ta4HfC5) is also considered as the most refractory material with the melting point over 4000 °C and valuable physical and mechanical properties. The main goal of this work is to fabricate TaC/HfCbased composites which consolidated by means of spark plasma...

In this research study, the effects of aluminum nitride (AlN) additive on the densification behavior and microstructure development of titanium diboride (TiB2) based ceramic matrix composite were investigated. In this way, a monolithic TiB2 ceramic and a TiB2–5 wt% AlN ultrahigh temperature ceramic composite were fabricated by spark plasma sintering (SPS) proces...

A facile one-pot aqueous solution method has been developed for the fast and straightforward synthesis of SnTe nanoparticles in more than ten gram quantities per batch. The synthesis involves boiling an alkaline Na₂SnO₂ solution and a NaHTe solution for short time scales, in which the NaOH concentration and reaction duration play vital roles in controlling the phase purity and particle size, re...

(Bi0.5Na0.5)TiO3 doped with 8 mol % BaTiO3 powder (BNT-BT0.08), prepared by sol-gel method was compacted and sintered by Spark Plasma Sintering (SPS) process. The influence of SPS temperature on the densification of BNT-BT0.08 ceramic was investigated. Starting from sol-gel nanopowder of BNT-BT containing 8 mol % BaTiO3 with an average particles size of about 30 nm, were obtained ceramics with ...

Alumina nanopowders produced by electrical explosion of wires were sintered using the spark plasma sintering technique. The results of XRD analysis show that the main phase in the compacted nanopowders is α-Al2O3. According to the SEM observations, the sintered alumina nanopowder consists of micron-sized faceted grains and nano-sized necked grains. The increase in sintering temperature resulted...

A transition from a low to a high spin state in the magnetization saturation between 1000 and 1100 oC calcination temperature is observed in YIG powders prepared by oxides mixture. Spark plasma sintering of these powders between 900 and 950 oC leads to dense samples with minimal formation of YFeO3, opening the way to cosintering of YIG with metals or metallic alloys. The optical properties depe...

Structural changes during the deformation-induced synthesis of nanocrystalline Fe-10Cr-3Al alloy powder via high-energy ball milling followed by annealing and rapid consolidation by spark plasma sintering were investigated. Reduction in crystallite size was observed during the synthesis, which was associated with the lattice expansion and rise in dislocation density, reflecting the generation o...

Silicon nitride foams were prepared by direct foaming and subsequent rapid sintering at 1600 °C. The intense thermal radiation generated under the pressureless spark plasma sintering condition facilitated necking of Si3N4 grains. The prepared foams possessed a porosity of ∼80 vol% and a compressive strength of ∼10 MPa, which required only ∼30 min for the entire sintering processes. Rapid growth...

Recently, local melting of the particle surfaces confirmed the formation of spark and plasma during spark plasma sintering, which explains the rapid densification mechanism via liquid. A model for rapid densification of flash sintered ceramics by liquid film capillary was presented, where liquid film forms by local melting at the particle contacts, due to Joule heating followed by thermal runaw...