Sulfur-containing solid electrolytes are highly attractive to scientists and increasing day by day. Recently, Li7P3S11, Li10GeP2S12, Li11Si2PS12 have been of great interest in literature. The ionic conductivity these can even be reached a value 10-2 S/cm. For this purpose, Li7P3S11 electrolyte is synthesized mechanical alloying method for all-solid-state Lithium Sulfur batteries study. To do th...

We have applied a novel 'melt synthesis technique' rather than a conventional solid-state reaction to rapidly synthesize phosphor materials. During a synthesis, the mixture of oxides or their precursors is melted by light pulses (10-60 s) in an arc-imaging furnace on a water-cooled copper hearth to form a globule of 1-5 mm diameter, which is then rapidly cooled by turning off the light. Using t...

A new synthesis route for phosphates in an organic solvent at low temperatures is presented. The synthesis was done by dispersing a nitrate salt and phosphorus pentoxide in dimethyl sulfoxide. The synthesis can be performed under water-free conditions and yielded several organic and inorganic phosphates. Crystal structure solution of bistetramethylammonium hydrogencyclotriphosphate, [N(CH3)4]2H...

The design principle and synthesis method of halide solid-state electrolytes are discussed in detail. Interface optimization their applications all-solid-state batteries described.

Chemistry is on the verge of a new era where the attention of chemists has shifted from covalent bonds to noncovalent interactions and their use as a reliable tool to design functional materials and to control the outcome of organic reactions. Although covalent synthesis in fluidic medium via supramolecular control has been achieved with limited success, the organic solid state has been of part...

in this work, all-solid-state potentiometric pvc membrane sensor was introduced for fast andsimple monitoring of mercury ions in waste water samples. the all solid sate electrode is made based on aconductive composite of graphite, reduced graphene oxide, epoxy resin on a copper wire. a thin layer pvcmembrane is then coated on the surface of the new conducting transducer. pvc membrane is compose...

In this paper, we used tetranuclear copper (II) Schiff base complexes, [Cu4 (μ-sal2hn) (μ-N3)2(N3)2] (1) and [Cu4 (μ-salophen) (μ1, 1-N3)2(N3)2] (2), as new precursor in solid-state thermal decomposition for the synthesis of CuO ...

a solid state fermentation method was developed for the production of citric acid from date pulp (obtained of date syrup production from the process) by aspergillus niger ptcc 5010. poor yield was obtained when potassium ferrocyanide treated date pulp were used as substrate, but methanol at a 3-4% concentration markedly increased the forma-tion of citric acid from the waste. the optimum range o...

in this work, ce0.75gd0.1ca0.15o1.8 nanopowders are successfully synthesized by a glycine-nitrate combustionprocess under the microwave irradiation. then calcination was carried out at 700 °c. calcined powdersidentified by room temperature x-ray diffraction were single phase and had a crystallite size between 16 to 24nm (based on schererr formula). scanning electron microscopy (sem) was employe...