نتایج جستجو برای: trace lead determination
تعداد نتایج: 641917 فیلتر نتایج به سال:
The paper describes an integrated luminometer able to perform fluorescence (FL), room temperature phosphorescence (RTP) and chemiluminescence (CL) measurements on seawater samples. The technical details of the instrumentation are presented together with flow injection (FI) manifolds for the determination of cadmium and zinc (by FL), lead (RTP) and cobalt (CL). The analytical figures of merit ar...
lead forms the complexes with xylenol orange in the basic solution. an adsorptivedifferential pulse stripping method for the determination of lead is proposed. the procedureinvolves an adsorptive accumulation of lead on a hanging mercury drop electrode (hmde) inthe presence of xylenol orange, followed by reduction of adsorbed lead by voltammetric scanusing differential pulse modulation. the opt...
abstract ion selective electrodes (ises) are electrochemical sensors that respond selectivity to the activity of ionic species. an ion-selective electrode is an electrochemical device that uses a thin selective membrane or film as the recognition element, and is an electrochemical half-cell equivalent to other half-cells of the zeroth (inert metal in a redox electrolyte). in common methods o...
INTRODUCTION The role of trace metals elements in human nutrition can no longer be ignored. Deficiency caused by inadequate dietary intake, secondary deficiencies often under - estimated, and iatrogenic deficiencies lead to pathologies such as infections and others. For this reason their dosages are particularly important to assess disease severity and to facilitate early treatment or improve p...
The present study describes a simple and highly selective method for separation, preconcentration and spectrophotometric determination of extremely low concentrations of lead. It is based on flotation of a complex of Pb(2+) ions and Alizarin yellow between aqueous and n-hexane interface at pH = 6. The proposed procedure is also applied for determination of lead in both tap water and prepared se...
An emission spectrochemical method is described for the determination of trace quantities of platinum, lead, and manganese in biological tissues. Total energy burns in an argon-oxygen atmosphere are employed. Sample preparation, conditions of analysis, and preparation of standards are discussed. The precision of the method is consistently better than +/- 15%, and comparative analyses indicate c...
A selective and sensitive method for simultaneous determination of lead and zinc by adsorptive differential pulse cathodic stripping voltammetry is presented. The method is based on adsorptive accumulation of the complexes of Pb (II) and Zn(II) ions with Dopamine onto hanging mercury drop electrode (HMDE), followed by reduction of adsorbed species by differential pulse cathodic stripping voltam...
The application of batch injection analysis to the determination of trace metals in samples of volume s 100 ~1 by square wave anodic stripping voltammetry has been investigated in detail, using a programmable electronic micropipette. The in situ formation of a mercury film on a glassy carbon electrode substrate, the influence of preconcentration time, injection rate and injected volume of analy...
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