A novel quantitative 1H NMR (Q-NMR) combined with HPLC-MS method has been proposed for investigating the degradation process of traditional Chinese medicine (TCM) components. Through this method, in-situ monitoring of dynamics degradation process of lithospermic acid (LA), one of the popular polyphenolic acids in TCM, was realized under low oxygen condition. Additionally, this methodology was p...

Background & Aims of the Study: In this study, 4-(2-pyridylazo) resorcinol (PAR) as model azo dye was used. In spectroscopic measurements and studies of PAR reagent as a ligand are used to formation a complex with toxic metals. So, removal and degradation these compounds of wastewaters are necessary. The aim of this study is the degradation of PAR from aqueous solutions in circulating fludized ...

In this research, ZnO nanoparticles (NPs) were synthesized using a binary Zn(II) Schiff-base complex. The complex heat-treated to prepare ZnO nanoparticles via thermal decomposition route at a temperature of 500 °C. The formation of single-phase ZnO nanoparticles and their microstructures were studied by XRD pattern, SEM and TEM observation. The photo-degradation characteristic of the as-prepar...

Degradation is a common problem for polymer matrix composites (PMCs) under low thermal cycling conditions. This paper investigates the effects of low thermal cycling on total mass loss (TML) and surface degradation of PMCs. Unnotched and open-hole specimens were weighed before and after low thermal cycling. The total mass loss and surface degradation of the specimens were studied over 250 cycle...

background: hydrocarbons degradation is principally achieved by microorganisms in natural environments. the extent of hydrocarbons biodegradation is mainly conditioned by environmental factors and its success depends on the optimal condition for the crude oil degrading isolates. objectives: the aims of the current study was to isolate and identify crude oil degrading bacterium from surface sedi...

We previously described a new iodinated vasopressin analogue (N epsilon-[125I]L-Tyr-[Lys8]-vasopressin) with high affinity for the vasopressin V1 and V2 isoreceptors. The aim of the present study was: i) to analyse the degradation pathway of N epsilon-[125I]L-Tyr-[Lys8]-vasopressin and (ii) to look for an effective inhibitor of radioligand degradation. N epsilon-[125I]L-Tyr-[Lys8]-vasopressin w...

Negative bias temperature instability (NBTI) has become a critical reliability phenomena in advanced CMOS technology. In this paper, we propose an analytical temperature-aware dynamic NBTI model, which can be used in two circuit operation cases: executing tasks with different temperatures, and switching between active and standby mode. A PMOS Vth degradation model and a digital circuits’ tempor...

This study investigates the effect of temperature on the ultrasonic degradation of polyvinyl acetate and polyvinyl chloride in chlorobenzene. The time evolution of molecular weight distribution was determined using gel permeation chromatography. Continuous distribution kinetics was used to obtain the degradation rate coefficients. The rate coefficients decrease with increasing temperature, and ...

Degradation of acrylic water base color from synthetic wastewater by the Fenton process was performed. Experiments were conducted on the sample containing 100 and 400 mg/l of Acrylic water base color. The study was performed for searching optimum values of FeSO4 and H2O2 concentration, pH and temperature. The H2O2 requirement seems to be re...

In this paper, a new methodology based on neural networks is proposed to study the thermal degradation process of some cholesteric liquid crystals decorated with ferrocene. First of all, a set of experimental data is obtained applying thermal analysis methods, under dynamic heating conditions. Neural networks were used to predict the thermostability (appreciated by the temperature when the degr...