In this study, simple, fast and reliable cyclic voltammetry (CV), linear sweep voltammetry (LSV), square wave voltammetry (SWV) and differential pulse voltammetry (DPV) methods were developed and validated for determination of bosentan in pharmaceutical preparations. The proposed methods were based on electrochemical oxidation of bosentan at platinum electrode in acetonitrile solution containin...

In this study, yttrium aluminum garnet (YAG) was prepared using a facile electrochemical technique. Four samples were synthesized in 0, 20, 40 and 60°C by electrochemical pulse deposition and were then calcined at 1200°C. The effect of synthesis temperature on morphology and structure of YAG was studied using X-ray diffraction, Fourier transform infrared spectroscopy and scanning electron micro...

The aim of this study was the preparation, characterization, and application of a multi-wall carbon nanotubes-epoxy composite electrode (MWCNT-EP) with 25%, wt. MWCNTs loading for the voltammetric/amperometric determination of pentachlorophenol (PCP) in aqueous solutions. The structural and morphological aspects of the MWCNT-EP composite electrode were examined by scanning electron microscopy. ...

Camptothecin (CPT) is a cytotoxic quinoline alkaloid endowed with the inhibition of topoisomerase I, an essential enzyme for the normal functioning of DNA. The redox behaviour of CPT was investigated at a glassy carbon electrode using cyclic, differential pulse and square wave voltammetry. It was shown that CPT can undergo reduction in a pH-dependent mechanism. In acid media only one irreversib...

A chemically modified carbon paste electrode with 2-chlorobenzoyl ferrocene (2CBF) and carbon nanotube (2CBFCNPE) was employed to study the electrocatalytic oxidation of ascorbic acid in aqueous solution using cyclic voltammetry, square wave voltammetry and chronoamperometry. The diffusion coefficient (D = 1.42 × 10-6 cm2 s-1), and the kinetic parameter such as ...