نتایج جستجو برای: cooling assisted microextraction

تعداد نتایج: 187182  

In this research, an analytical method for quantification of the thermal energy performance improvement for a building integrated photovoltaic double-skin façade has provided. The system has been suggested as a retrofit measure for an existing building in Tehran. The effect of thermal performance has been analyzed through computer-assisted developed code using engineering equation solver softwa...

Journal: :Analytical sciences : the international journal of the Japan Society for Analytical Chemistry 2009
Rie Ito Migaku Kawaguchi Youji Koganei Hidehiro Honda Noriya Okanouchi Norihiro Sakui Koichi Saito Hiroyuki Nakazawa

A simple and highly sensitive method that involves miniaturized hollow fiber assisted liquid-phase microextraction (HF-LPME) with in situ acyl derivatization and GC-MS was developed for the determination of benzophenone (BP) and related compounds in human urine samples. The limits of detection (S/N = 3) and quantification (S/N > 10) of BPs in human urine samples are 0.01 to 0.05 and 0.05 to 0.2...

Journal: :analytical and bioanalytical chemistry research 2014
mir ali farajzadeh leila khoshmarram saheleh sheykhizadeh

foodstuffs analysis is very important due to population growth and increasing consumer demand for safety and nutritional excellence. the analysis of different compounds in foodstuffs is so difficult without using sample preparation techniques. traditional techniques require large amounts of toxic organic solvents. as a result, they are not only expensive but also environmentally unfriendly and ...

Journal: :Journal of the American Society for Mass Spectrometry 2016
Mandy S Phelps Drew Sturtevant Kent D Chapman Guido F Verbeck

We describe a novel technique combining precise organelle microextraction with deposition and matrix-assisted laser desorption/ionization (MALDI) for a rapid, minimally invasive mass spectrometry (MS) analysis of single organelles from living cells. A dual-positioner nanomanipulator workstation was utilized for both extraction of organelle content and precise co-deposition of analyte and matrix...

2016
AkbAR AkbARI

A new, rapid and highly sensitive and rapid method was proposed for the simultaneous determination trace levels of vitamin C and folic acid in the human urine samples. The inûuence affecting factors on the UA-DLLME such as type and volume of the dispersive and extraction solvent, pH, ionic strength and temperature of sample solution, sonication condition investigated and optimized. Under the op...

2017
Ya-Bing Xiong Yue Zhao Zhong-Hua Yang

A novel, rapid and efficient manual shaking and ultrasound-assisted surfactant-enhanced emulsification microextraction (M-UASEME) combined with gas chromatography-flame photometric detection (GC-FPD) was developed for the extraction and determination of eight organophosphorus pesticides (OPPs) in tap water and honey samples. The main parameters that affected the extraction efficiency were inves...

Journal: :Analytical sciences : the international journal of the Japan Society for Analytical Chemistry 2010
Sayed Zia Mohammadi Daryoush Afzali Yar Mohammad Baghelani

In the present work, a new ligandless-ultrasound-assisted emulsification microextraction (LL-USAEME) method was developed for preconcentration trace amounts of nickel as a prior step to its determination by flame atomic absorption spectrometry. Some factors influencing the extraction efficiency of nickel and its subsequent determination were studied and optimized, such as type and volume of the...

Journal: :Processes 2021

This paper would like to compare two extraction procedures for analyzing phthalates (PAEs) in hot drinks collected at vending machines, usually coffee and tea. The analytical are based on Solid Phase Extraction (SPE) using C18 cartridge dispersive liquid-liquid microextraction (DLLME) assisted by ultrasound vortex improving the dispersion mechanically, with each followed a routinary method such...

Journal: :Cryobiology 2011
M Sansinena M V Santos N Zaritzky J Chirife

Oocyte cryopreservation is of key importance in the preservation and propagation of germplasm. Interest in oocyte cryopreservation has increased in recent years due to the application of assisted reproductive technologies in farm animals such as in vitro fertilization, nuclear transfer and the need for the establishment of ova/gene banks worldwide. However, the cryopreservation of the female ga...

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