نتایج جستجو برای: Low temperature synthesis

تعداد نتایج: 1923025  

پایان نامه :وزارت علوم، تحقیقات و فناوری - دانشگاه رازی - دانشکده علوم 1390

in this thesis, a better reaction conditions for the synthesis of spirobarbiturates catalyzed by task-specific ionic liquid (2-hydroxy-n-(2-hydroxyethyl)-n,n-dimethylethanaminium formate), calcium hypochlorite ca(ocl)2 or n-bromosuccinimide (nbs) in the presence of water at room temperature by ultrasonic technique is provided. the design and synthesis of spirocycles is a challenging task becaus...

پایان نامه :وزارت علوم، تحقیقات و فناوری - دانشگاه رازی - دانشکده علوم 1390

abstract in first part of this project, the use of a new and biguanid-like catalyst supported on silica as a recyclable catalyst provides a new route for the synthesis of a variety of arylalkylidene rhodanine derivatives through knoevenagle reaction in at present of solvent at room temperature. rhodanine derivatives and especially arylalkylidene rhodanines have proven to be attractive compound...

Journal: :international journal of bio-inorganic hybrid nanomaterials 0

nanostructured zinc oxide (zno) materials have received considerable interest from scientists due to their remarkable performance in electronics, optics and photonics. zno nanoparticles were synthesized by co-precipitation method. zno nanoparticles were synthesized using zn(no3)3 and k2co3 precursors. the structure of the obtained product was confirmed by the powder x-ray diffraction (xrd) anal...

A. Beitollahi1, B. Alinejad1,, H. Sarpoolaky1,, S. Afshar2,

Abstract: Nanocrystalline MgAl2O4 spinel powder was synthesized using metal nitrates and a polymer matrix-based composed of sucrose and polyvinyl alcohol (PVA). The precursor and the calcined powders were characterized by simultaneous thermal analysis (STA), X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), and scanning electron microscopy (SEM). According to XRD res...

F. Golestani-Fard, F. Khorasanizadeh, M. Aminzare, S. Zhang, Y. Safaei-Naeini,

Abstract: composition of MgO and nano boehmite. The reactant and potassium chloride, as the reaction media, were fired at800-1000 °C at different dwell times (0.5-5 h) in the ambient atmosphere. After washing and filtration, the spinel nanopowder was characterized by X-ray diffraction (XRD), Scanning electron microscopy (SEM), and Brunauer-Emmett-Teller (BET) techniques. It was demonstrated tha...

Journal: :international journal of nanoscience and nanotechnology 2008
anal k. jha k. prasad and a. r. kulkarni

a green low-cost and reproducible yeast mediated synthesis of silver nanoparticles is reported. the synthesis is performed at room temperature. x-ray and transmission electron microscopy analyses are performed to ascertain the formation of ag nanoparticles. nanoparticles almost spherical in shape having a size of 6-20 nm are found.

Journal: :international journal of nanoscience and nanotechnology 2010
s. mohammadkhani m. aghaziarati

in this research, a single-stage low-temperature hydrothermal synthesis route was successfully developed for preparation of iron disulfide. the prepared powder was characterized by x-ray diffraction (xrd) and scanning electron microscopy (sem). these analyses showed that nanoparticles were well crystallized, pyrite was the main product and the shape of crystals was nanorod. also, the influences...

Journal: :journal of ultrafine grained and nanostructured materials 2015
mehdi hamdam momen mahmoud heydarzadeh sohi ahmadali amadeh

in this study, a novel method called “atmospheric pressure solution evaporation (apse)” wasdeveloped for growing of zinc oxide (zno) nanostructures on al2o3 surface. zinc acetate dihydrate,polyvinyl pyrrolidone, and deionized water were used as precursor, capping, and solvent, respectively.the growth of zno nanostructures from evaporated solution was performed at three temperatures of300, 400, ...

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