This paper presents a novel microwave-assisted hydrothermal technique for synthesizing tin(II) oxide nanoparticles. This technique can be used for producing large quantities of homogeneous nanoparticles in a short time. The effect of the solution molarity, final pH, hydrothermal processing time and microwave power were studied. The tin(II) oxide structure verified from XRD...

in the past decades, many methods have been developed to synthesize zero- dimensional  nanoparticles, quasi–one–dimensional (1d) cuo nanostructures, such as metal organic deposition technique,  microwave irradiation, sol-gel-like dip  technique, reverse micelle-assisted route, chemical method, and simple template free solution route. among those synthesis methods, hydrothermal and chemical reac...

In this report, a technique for rapid synthesis of ZnO microstructures by microwave-assisted heating of precursors at hydrothermal conditions is demonstrated. Further, the reaction mechanism for the growth of ZnO microstructures is analyzed. An accelerated rate of reaction obtained using microwaves enables a dissolution-recrystallization mechanism for generation of one dimensional (1D) rod-like...

In the past decades, many methods have been developed to synthesize zero- dimensional  nanoparticles, quasi–one–dimensional (1D) CuO nanostructures, such as metal organic deposition technique,  microwave irradiation, sol-gel-like dip  technique, reverse micelle-assisted route, chemical method, and simple template free solution route. Among those synthesis methods, hydrothermal and chemical reac...

In the past decades, many methods have been developed to synthesize zero- dimensional  nanoparticles, quasi–one–dimensional (1D) CuO nanostructures, such as metal organic deposition technique,  microwave irradiation, sol-gel-like dip  technique, reverse micelle-assisted route, chemical method, and simple template free solution route. Among those synthesis methods, hydrothermal and chemical reac...

11 12 Abstract Nanorods and nanoplates of Y2O3:Eu 3+ powders 13 were synthesized through the thermal decomposition of the 14 Y(OH)3 precursors using a microwave-hydrothermal meth15 od in a very short reaction time. These powders were 16 analyzed by X-ray diffraction, field emission scanning 17 electron microscopy, Fourrier transform Raman, as well as 18 photoluminescence measurements. Based on ...

semiconductor nanoparticles exhibit size dependent properties due to quantum confinement effect that arenot present in their bulk counterparts. in this work, extremely fine and pure sno2 nanoparticles of ~1.1nm size were synthesized by a solution process, in which amorphous precipitate of sno2 was crystallizedby microwave heating. the particles sizes varied from ~1.1 to ~2.7 nm. by xrd analysis...

A micro-sheet anatase TiO(2) single crystal photocatalyst with a remarkable 80% level of reactive {001} facets was synthesized via a microwave-assisted hydrothermal route involving titanium tetrafluoride and a tetrafluoroborate-based ionic liquid.

perlite or pearl stone is a natural glass which has formed by rapid cooling of viscous lava or magma. perlite is mainly composed of silica, aluminum, potassium and sodium. in this experiment, perlite was used as a low-cost source of si and al to synthesis of sodalite zeolite using the alkaline hydrothermal treatment. a statistical taguchi design of experiments was employed to evaluate the effec...

Perlite or pearl stone is a natural glass which has formed by rapid cooling of viscous lava or magma. Perlite is mainly composed of silica, aluminum, potassium and sodium. In this experiment, perlite was used as a low-cost source of Si and Al to synthesis of sodalite zeolite using the alkaline hydrothermal treatment. A statistical Taguchi design of experiments was employed to evaluate the effec...