the aim of this study was to investigate the sol gel synthesis of ha/fa nanoparticles and the possible formation of tcp phase or unstoichiometric calcium deficient hydroxyapatite (cdha) from the precursors with a ca/p ratio of 1.62. in order to prepare the sol, the solutions of triethyl phosphite, ammonium fluoride and calcium nitrate in ethanol were used respectively as p, f and ca precursors....

The aim of this study was to investigate the sol gel synthesis of HA/FA nanoparticles and the possible formation of TCP phase or unstoichiometric calcium deficient hydroxyapatite (CDHA) from the precursors with a Ca/P ratio of 1.62. In order to prepare the sol, the solutions of Triethyl phosphite, ammonium fluoride and calcium nitrate in ethanol were used respectively as P, F and Ca precursors....

The aim of this study was to investigate the sol gel synthesis of HA/FA nanoparticles and the possible formation of TCP phase or unstoichiometric calcium deficient hydroxyapatite (CDHA) from the precursors with a Ca/P ratio of 1.62. In order to prepare the sol, the solutions of Triethyl phosphite, ammonium fluoride and calcium nitrate in ethanol were used respectively as P, F and Ca precursors....

Aligned porous non-sintered and sintered a-tricalcium phosphate (a-TCP) scaffolds are prepared by ice-templating converted into the low-temperature calcium phosphates calcium-deficient hydroxyapatite (CDHA), brushite monetite. This is achieved hydrothermal treatment or incubation in phosphoric acid solution has a high clinical potential due to higher solubility of these phases. Further details ...

Multiphasic calcium phosphate powders were synthesized by the acidic route, using lactic acid as a chelating agent that allows production of stable and rich solution ions at room temperature. After pH adjusting, without varying concentrations precursor solution, XRD FTIR analyses showed different CaP phases before after heat treatment 1000 °C. At 5, brushite plate-like particles produced, while...

Ultrafine individualised mono crystalline Ca(10-x)(PO4)(6-x)(HPO4)x(OH)(2-x) deficient calcium hydroxyapatite nanocrystals displaying fluorescence under visible excitation are proposed for utilisation as biocompatible biological probes.

In this study, the effects of sodium lauryl sulfate and various amino acids (DL-aspartic acid, dodecanedioic suberic acid) on formation calcium-deficient hydroxyapatite via hydrolysis α-tricalcium phosphate (α-TCP) were investigated; moreover, a combined effect these additives ethylene glycol as synthesis medium was also estimated. The reaction performed in solutions containing different concen...

A range of crystalline and nano-sized carbonate- and silicate-substituted hydroxyapatite has been successfully produced by using continuous hydrothermal flow synthesis technology. Ion-substituted calcium phosphates are better candidates for bone replacement applications (due to improved bioactivity) as compared to phase-pure hydroxyapatite. Urea was used as a carbonate source for synthesising p...