نتایج جستجو برای: indicating method

تعداد نتایج: 1791594  

Journal: :iranian journal of pharmaceutical research 0
zengkun xie southwest university lihua wei southwest university qin yang southwest university min yang southwest university hongchun pan southwest university hong liu southwest university

the objective of the study was to develop a simple, specific and stability-indicating hplc method for the simultaneous determination of creatine phosphate sodium (cps) and its related substances in pharmaceutical formulation. separation of creatine phosphate sodium from its major process impurities and degradation products was achieved on a hypersil bds c18 column (250 × 4.6 mm, 5 μm) with an a...

Journal: :IEEJ Transactions on Electronics, Information and Systems 1987

2014
Ranjeet Kumar T. Rama Mohan Reddy

High performance liquid chromatography (HPLC) is an integral analytical tool in assessing drug product stability. HPLC methods should be able to separate, detect, and quantify the various drug-related degradants that can form on storage or manufacturing, plus detect and quantify any drug-related impurities that may be introduced during synthesis. Forced degradation studies of new chemical entit...

Journal: :Bulletin of Pharmaceutical Sciences. Assiut 2005

2009
K.Srinivasa Rao M. Sunil

A novel stability-indicating high-performance liquid chromatographic assay method was developed and validated for valacyclovir in the presence of degradation products generated from forced decomposition studies. A Hypersil ODS C-18 (250 x 4.6 mm, packed with 5 micron) column in an isocratic mode with the mobile phase acetonitrile: phosphate buffer (pH3.6) (50:50%v/v) was used. The flow rate was...

A simple and rapid stability indicating method based on capillary zone electrophoresis has been developed and validated for the analysis of buserelin (BUS). The best separations were achieved by using a bare fused silica capillary (75 m i.d.; 65.5 cm total, 57.0 cm effective length), phosphate buffer (pH = 3.00; 26.4 mM), at 35 °C. The sample was hydrodynamically injected at 50 mbar for 5 seco...

Journal: :International Journal of Current Pharmaceutical Research 2017

A simple and rapid stability indicating method based on capillary zone electrophoresis has been developed and validated for the analysis of buserelin (BUS). The best separations were achieved by using a bare fused silica capillary (75 m i.d.; 65.5 cm total, 57.0 cm effective length), phosphate buffer (pH = 3.00; 26.4 mM), at 35 °C. The sample was hydrodynamically injected at 50 mbar for 5 seco...

Journal: :iranian journal of pharmaceutical research 0
elnaz tamizi tabriz university of medical sciences ernst kenndler institute for analytical chemistry, faculty of chemistry, university of vienna, a 1090 vienna. waehringerstrase 38, vienna, austria abolghasem jouyban faculty of pharmacy

a simple and rapid stability indicating method based on capillary zone electrophoresis has been developed and validated for the analysis of buserelin (bus). the best separations were achieved by using a bare fused silica capillary (75 m i.d.; 65.5 cm total, 57.0 cm effective length), phosphate buffer (ph = 3.00; 26.4 mm), at 35 °c. the sample was hydrodynamically injected at 50 mbar for 5 seco...

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