The microstructure and morphology of solid-oxide fuel-cell electrodes are very complex but important because they strongly affect the electrical performance of the cell. In this work the high-resolution X-ray nanotomography technique is applied to reconstruct the three-dimensional microstructure of a (La(0.8)Sr(0.2))(0.95)MnO(3) yttria-stabilized zirconia composite cathode. Some key microstruct...

Diierent bounds on the conductivity of a composite material may improve on each other in diierent conductivity regimes. If so, the question arises of how to eeciently interpolate between the bounds. In this paper we show how to do an interpolation with a two-point Pad e approximation method. For bounds on two-component composites the interpolation method is shown to be, in a sense, the best pos...

a hydrothermal method for preparation of nano-size zirconia has been studied to optimize the effective parameters (precursor concentration, temperature and time) using response surface methodology (rsm). the synthesized zirconia samples were characterized through x-ray diffraction (xrd), scanning electron microscope (sem) and transmission electron microscopy (tem) analyses to identify mean nano...

Crystal structure and compressibility of potassium azide was investigated by in-situ synchrotron powder X-ray diffraction in a diamond anvil cell at room temperature up to 37.7 GPa. In the bodycentered tetragonal (bct) phase, an anisotropic compressibility was observed with greater compressibility in the direction perpendicular to the plane containing N3 ions than directions within that plane. ...

objective: a clinical challenge of using zirconia frameworks is to achieve adequate bond with different substrates. this study aimed to evaluate the effect of bioglass and silica coating of zirconia substrates on microshear bond strength of resin cement to tetragonal zirconia. methods: this laboratory experimental study was conducted on zirconia discs. a total of 120 ytzp zirconia (zirkonzahn) ...

Alumina/zirconia (Al2O3/ZrO2) multilayer thin films were deposited on Si (100) substrates at an optimized oxygen partial pressure of 3 Pa at room temperature by pulsed laser deposition. The Al2O3/ZrO2 multilayers of 10:10, 5:10, 5:5, and 4:4 nm with 40 bilayers were deposited alternately in order to stabilize a high-temperature phase of zirconia at room temperature. All these films were charact...

A hydrothermal method for preparation of nano-size zirconia has been studied to optimize the effective parameters (precursor concentration, temperature and time) using response surface methodology (RSM). The synthesized zirconia samples were characterized through X-ray diffraction (XRD), scanning electron microscope (SEM) and transmission electron microscopy (TEM) analyses to identify mean nano...

Porous yttria-stabilised zirconia ceramics have been gaining popularity throughout the years in various fields, such as energy, environment, medicine, etc. Although yttria-stabilised zirconia is a well-studied material, voided yttria-stabilised zirconia powder particles have not been demonstrated yet, and might play an important role in future technology developments. A sol-gel synthesis accomp...

Abstract: Zirconia solid electrolytes with nonequilibrium composite structure were prepared by impregnation of a porous 8YSZ matrix with a solution of Zirconia. Microstructures were characterized by XRD and SEM. The electrical properties were studied by impedance spectroscopy as a function of temperature. Biaxial flexural strength and fracture toughness of composite samples were measured by rin...