نتایج جستجو برای: 99 standard method with hexane and acetone solvents
تعداد نتایج: 18593444 فیلتر نتایج به سال:
we describe here a suitable approach for the synthesis of n-unsubstituted monocyclic b-lactams under mild reaction conditions by the annelation of imines with substituted acetylchlorides. in this method the reaily available phtalimidoacetyl chloride were allowed to react with - dibenzylideneiminotoluene (hydrobenzamide) in the presence of an equimolar amount of triethylamine in refluxing toluen...
We investigated the determination of N-methylcarbamate pesticides and their metabolites in agricultural products by HPLC with post-column fluorescence detection after clean-up with an SPE cartridge. The homogenate of agricultural products was extracted with acetone. The crude extract was partitioned between 5% sodium chloride solution and dichloromethane, and the dichloromethane layer was conce...
Plants extracts has been used in traditional medicine for many years. The use of them has the least side effects in comprison to the synthetic drugs. The aim of this study was investigation and comparision of biological active components of Quercus persica and Quercus ilex. Sampling was done from Quercus persica and Quercus ilex stands. The antibacterial activity was assayed against Psuodomonas...
Plants extracts has been used in traditional medicine for many years. The use of them has the least side effects in comprison to the synthetic drugs. The aim of this study was investigation and comparision of biological active components of Quercus persica and Quercus ilex. Sampling was done from Quercus persica and Quercus ilex stands. The antibacterial activity was assayed against Psuodomonas...
The diffusion behavior of methanol in different critical media (n-pentane, n-hexane, n-heptane and acetone) was investigated by the Monte Carlo (MC) method. From the simulation results, the diffusion constant of methanol molecule in the critical n-hexane is much larger than those in n-pentane, n-heptane and acetone. By analyzing the microscopic configurations of the critical mixtures, it is fou...
A sensitive and selective analytical method for the determination of pindone in agricultural products by LC-MS/MS was developed. Pindone was extracted with acetone, and an aliquot of the crude extract was re-extracted with hexane. For lipid-rich samples, the crude extract was further cleaned up by acetonitrile-hexane partitioning. The extract was cleaned up on a tandem graphitized carbon-silica...
The larvicidal potential of different solvent crude (hexane, chloroform, ethyl acetate, acetone and methanol) leaf extracts of four plants (Blepharis maderaspatensis, Elaeagnus indica, Maesa indica, Phyllanthus wightianus and Memecylon edule) was tested against the fourth-instar larvae of Aedes aegypti. Insecticidal susceptibility tests were carried out using WHO standard method and the mortali...
Dispersive Liquid-Liquid MicroExtraction technique based on Solidification of a Floating Organic drop (DLLME-SFO) combined with flame atomic absorption spectrometry was developed for determination of thallium in water sample. An appropriate mixture of acetone and 1-undecanol was rapidly injected into an aqueous sample containing TlCl4- which forms an ion pair with bril...
today the image of a permanent skeletal space of cities affected by some forces or mechanisms is put in time with social-economic development and while imposes a new face and perspective to physical anatomy of cities, and prepares field to changes in content and social- economic structures of cities too. simultaneously with quitting villages in order to settle in cities by villagers, the phen...
dibutyl phthalate (dbp) is a phthalic acid ester and is widely used in polymeric products to make them more flexible. dbp is found in almost every plastic material and is believed to be persistent in the environment. various analytical methods have been used to measure dbp in different matrices. considering the ubiquitous nature of dbp, the most important challenge in dbp analyses is the contam...
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