a novel potentiometric ion-selective pvc membrane sensor for analysis of atorvastatin (at) in pharmaceutical preparations based on atorvastatin-(tetraphenyl borate), (at-(tpb)2) as sensing element, tetraphenyl borate as additive and tris-2-ethyl-hexyl phosphate (top) as plasticizer solvent was prepared. the electrode shows a good nernestian response over the concentration range of 0.09–5586 µg ...

A stopped flow rapid reaction apparatus capable of following changes of +/-0.02 pH unit in 0.1 ml of solution in less than 0.005 sec has been developed, utilizing a commercially available pH-sensitive glass electrode. Using this instrument, extracellular pH at 37 degrees C was followed from less than 0.025 sec to 300 sec after mixing equal volumes of the following CO(2)-free solutions: (A) norm...

an iodide ion-selective pvc membrane sensor based on copper (π)-bis-nphenilsalicyldenaminatocomplex as a novel sensing material is successfully developed. theelectrode showed a good selectivity for iodide ion with respect to common inorganic anions. thesensor exhibited a good linear response with slope of _58.6 ± 0.4 mv per decade over theconcentration range of 5.0 × 10-6 to 1.0 × 10-1 mol l-1,...

OBJECTIVE To investigate and compare the amount of fluoride release of conventional, resin modified and nanofilled resin modified glass ionomer cements. MATERIALS AND METHODS Tablets of glass-ionomer cements were immersed in deionized water and incubated at 37°C. After 1, 2, 7, 15 and 30 days, fluoride ion was measured under normal atmospheric conditions by fluoride ion selective electrode. B...

IN the course of an investigation into the value of the glass electrode as a means of making continuous records of the hydrogen ion concentration of circulating blood, it was found, in the preliminary experiments in which estimations were made on single samples, that there were several sources of serious error. The difficulties encountered in devising a satisfactory apparatus for measuring glas...

Quantitative extracellular electrical stimulation data were obtained from single fibers in the dorsal columns of anesthetized and paralyzed cats. Single-fiber responses were recorded with glass microelectrodes. The threshold current was found for fibers stimulated with a 100-p diameter monopolar electrode at the surface of the dorsal columns 0.5-2.0 cm from the recording electrode. Shock artifa...

a new poly(vinylchloride) membrane sensor for cr3+ ions based on di (benzylamino)glyoxime asan ionophore was prepared. the electrode has a linear dynamic range 1×10-6-1×10-1 mol l-1,with anernstian slope of 20.3 ± 0.5 mv per decade and a detection limit of 2×10-7. it has a fast responsetime of