ticl4, ammonia, inorganic salts as raw material, nanometer composite-crystal tio2 powders were synthesized by two-step chemical method. precursors were crystallized with different phase and stable composite-crystal tio2 with anatase and rutile phase was prepared at low temperature. quantitative control of crystal phase was realized. remarkable factors including reaction ph value, reaction time,...

TiCl4, ammonia, inorganic salts as raw material, nanometer composite-crystal TiO2 powders were synthesized by two-step chemical method. Precursors were crystallized with different phase and stable composite-crystal TiO2 with anatase and rutile phase was prepared at low temperature. Quantitative control of crystal phase was realized. Remarkable factors includ...

alumina nanomaterials were synthesized via a solution combustion technique using tris-(acetylacetonato) aluminum(iii) complex (1) and tris-(2-formylphenolate) aluminum(iii) complex (2) at 600, and 1000 °c for 3h. the obtained data showed that the procedure without using fuel resulted in a better phase and morphology. to investigate the phase formation, powder x-ray diffraction technique was use...

nano-sized titanium dioxide tio2 powder was successfully prepared from its precursor titanium (iv) chloride by a simple and new wet chemical method. ticl4 were used as precursor in hydrogen peroxide, h2o2 and ethanol. this solution was then peptized using nitric acid and heated under reflux at 80°c. their physico-chemical properties were then characterized by transmission electron microscopy (t...

In a ring laser gyroscope, due to the rotation and the Sagnac effect, a phase difference between the two counter-propagating beams is generated. In this device, the higher phase difference between these two beams causes the better the interference pattern detection, and thus the sensitivity is increased. In this paper, the effect of inserting a dielectric-graphene photonic crystal inside a ring...

Sub-micrometer-sized CdS spheres were synthesized by hydrothermal and solvothermal reactions using Cd(NO3)2.4H2O and CH4N2S raw materials at a constant stoichiometric 1 : 2, Cd : S molar ratio. Various conditions such as solvent type (water and/or ethanol), reaction time and temperature were examined for the synthesis of the targets. The sy...

Different crystal phase with a same chemical structure, polymorphous, is a specific physical characteristic which determine the end usage of pigments especially in high performance ones. Diketopyrrolopyrrole DPP derivatives, as one of the innovative in heterocyclic pigments, follow this pattern. Synthesis of pigment red 254 in selected crystal phase using ionic liquids was achieved without any ...

Sub-micrometer-sized CdS spheres were synthesized by hydrothermal and solvothermal reactions using Cd(NO3)2.4H2O and CH4N2S raw materials at a constant stoichiometric 1 : 2, Cd : S molar ratio. Various conditions such as solvent type (water and/or ethanol), reaction time and temperature were examined for the synthesis of the targets. The sy...

Nanostructured Ni2As2O7 semiconductor samples were synthesized by a solid state method among As2O3 and Ni(NO3)2.6H2O raw materials at 650 °C (S1) and 750 °C (S2) as reaction temperatures. The synthesized nanomaterials were characterized by powder X-ray diffraction (PXRD) technique and F...

Alumina nanomaterials were synthesized via a solution combustion technique using tris-(acetylacetonato) aluminum(III) complex (1) and tris-(2-formylphenolate) aluminum(III) complex (2) at 600, and 1000 °C for 3h. The obtained data showed that the procedure without using fuel resulted in a better phase and morphology. To investigate the phase formation, powder X-ray diffraction technique was use...