نتایج جستجو برای: room temperature
تعداد نتایج: 510139 فیلتر نتایج به سال:
in this thesis, a better reaction conditions for the synthesis of spirobarbiturates catalyzed by task-specific ionic liquid (2-hydroxy-n-(2-hydroxyethyl)-n,n-dimethylethanaminium formate), calcium hypochlorite ca(ocl)2 or n-bromosuccinimide (nbs) in the presence of water at room temperature by ultrasonic technique is provided. the design and synthesis of spirocycles is a challenging task becaus...
abstract in first part of this project, the use of a new and biguanid-like catalyst supported on silica as a recyclable catalyst provides a new route for the synthesis of a variety of arylalkylidene rhodanine derivatives through knoevenagle reaction in at present of solvent at room temperature. rhodanine derivatives and especially arylalkylidene rhodanines have proven to be attractive compound...
1- in a search directed to the reaction of compound)23(the cycloaddition reaction of 1,3- diphenylisobenzofurane)14(with p-benzoquinone)19(,followed by addition of cyclopentadiene was carried out.the specific spacial stracture of its ir,nmr,mass spectra. 2- in another attempt the kinetic stability and behavior of compounds)20(and)23(was studied.the main subject of this study was the highly reve...
phenolic resin is among the oldest thermoset resins that have found wide spread applications in several industries, largely due to its high thermal resistance. in this research, room temperature curing of phenolic resin and its reinforced silica composite has been investigated by p-toluene sulphonic acid as a catalyst. mechanical properties of the composites such as impact strength, flexural pr...
in this research, the survival of probiotic microorganisms in yogurts stored at room temperature (cold chain interruption conditions) was studied. milk inoculated with yogurt bacteria (mixed culture of streptococcus thermophilus and lactobacillus delbrueckii ssp. bulgaricus) and a single probiotic culture (l. acidophilus la-5 or bifidobacterium lactis bb-12 or l. rhamnosus hn001 or l. paracasei...
the magnetically recoverable fe3o4 nanoparticle and the supported brønsted acidic ionic liquid 1-methyl-3-(3-trimethoxysilylpropyl) imidazolium hydrogen sulfate (fe3o4-il-hso4) were synthesized and used as efficient magnetic catalysts for the regioselective thiocyanation of aromatic and heteroaromatic compounds at room temperature in water: ethanol. this procedure provided the target thiocyanat...
simple, low temperature and environmentally benign green route is proposed for preparation of nanocrystalline zno in presence of a low-cost and halide-free room-temperature ionic liquid (rtil) by refluxing at 95 °c for 60 minutes. the x-ray diffraction (xrd) studies display that the products are well-crystallized in the form of wurtzite hexagonal. morphology of the as-prepared zno was character...
in this research, we have developed cheap recyclable and task-specific acidic ionic liquids (ails) 1-hydrogen-3-methylimidazolium hydrogen sulfate [hmim]hso4, 1-hydrogen-3-methylimidazolium chloride [hmim]cl, 2-pyrrolidonium hydrogensulfate [hnhp]hso4 and applied them in acid catalyzed synthesis of quinoxaline derivatives from 1,2-phenylendiamines and 1,2-dicarbonyl compounds. the products coul...
the knoevenagel condensation of aromatic aldehydes with barbituric acid, dimedone and malononitrile occurred in the presence of bf3/nano-γ-al2o3 at room temperature in ethanol. this catalyst is characterized by powder x-ray diffraction (xrd), fourier transform infrared spectroscopy (ft-ir), thermal gravimetric analysis (tga), field emission scanning electron microscopy (fesem) and energy-disper...
methanesulfonic acid (msa) was found to be an efficient catalyst for the synthesis of 1-substituted-1h-1,2,3,4-tetrazoles. a series of 1-substituted tetrazole compounds were synthesized from the reaction of various primary amines, sodium azide and triethyl orthoformate in the presence of catalytic amounts of msa at room temperature. in this protocol, some of the tetrazole derivatives were synth...
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