Si3N4/BN fibrous monoliths were prepared with 4 wt% Y2O3 added as a sintering aid to the Si3N4. Residual carbon, present in the billet before hot-pressing, was shown to influence the final microstructure. The sintering aid glass, known to migrate into the BN cell boundaries during hotpressing, was not sufficient in quantity to prevent premature shear failure when samples were tested in flexure....

Hot-pressing was used to prepare a dense (97% relative density) cubic Al substituted Li7La3Zr2O12 material at temperatures lower than typically used for solid-state and/or liquid phase sintering. Electron microscopy analysis revealed equiaxed grains, grain boundaries, and triple junctions free of amorphous and second phases and no Al segregation at grain boundaries. These results suggest that A...

In this study, an industrial polycrystalline SiC tile was successfully sintered by pressureless sintering at 2150°C for 1 hour. The physical and mechanical properties of silicon carbide including density, hardness, bending strength, and fracture toughness were evaluated. The results indicated that the mentioned properties were 3.08 g.cm-3, 2503 HV0, 249.3 MPa, and 1.23 MPam0.5</...

Alumina-Mullite-Zirconia ceramic composites were prepared by reaction sintering of alumina, zircon mixture and the sintering aids of magnesia and titania at temperatures of 1400 and 1600 C for 2 hours. The development of different phases and microstructures of the composites were analysed to assess the relative influence of the additives on the formation of alumina-zirconia-mullite compos...

In this study, a combustion synthesized AlN powder was sintered using microwave as heating source. The microwave was 2.45 GHz and the sintering process was carried out in a single-mode cavity. The sintering temperature was between 1800°C and 2000°C with a power ranging from 400 to 700W. The as-synthesized AlN was ground to under 2μm and yttria was used as sintering aid. The effects of the amoun...

Low-melting H3BO3, acting as sintering aid, was used to reduce the sintering temperature of 5 wt.% CaTiO3-doped (Zn0.65Mg0.35)TiO3 ceramics. The sintering behaviors, microstructures and microwave dielectric properties with different amounts of H3BO3 addition were investigated. The results showed that H3BO3 additive was very effective for lowering the sintering temperature and improving the bulk...

Garnet-type solid electrolytes have attracted extensive attention for solid-state lithium (Li) batteries. However, the high processing temperature of up to 1,200°C limits large-scale production. Here, we report a simple approach reduce sintering by using conformal nanoscale amorphous alumina coating. The ceramic sintered at 980°C shows room ionic conductivity 0.13 mS cm?1. It reveals that secon...

When traditional sintering techniques are used it is difficult to obtain dense materials with nanometric or submicrometric grain sizes. Microwave sintering was proposed as an alternative technique to overcome the problems of conventional fast heating. However, various problems usually occur when ceramics are sintered by direct microwave heating [1]. Hybrid heating techniques, which combine dire...

Si2N2O is considered as a new great potential structural/functional candidate in place of Si3N4. The amorphous Si3N4 nanopowder was incorporated into silica sol by adding of MgO and Y2O3 as sintering aid. Synthesized powders were heated by spark plasma sintering at a heating rate of 100 oC/min yielded fully dense compacts at 1550 and 1750 oC for 40 min. The phase formation of samples was charac...